Bis(triphenylphosphine)copper(I) nitrate

Base Information

• Chemical Name: Bis(triphenylphosphine)copper(I) nitrate
• CAS No.: 106678-35-7
• Molecular Formula: C₃₆H₃₀CuP₂*NO₃
• Molecular Weight: 650.133
• European Community (EC) Number: 631-247-8,636-613-0
• DSSTox Substance ID: DTXSID20558957
• Mol file: 106678-35-7.mol

Synonyms:106678-35-7;Bis(triphenylphosphine)copper(I) nitrate;BIS(TRIPHENYLPHOSPHINE)COPPER (I) NITRATE;copper(1+);triphenylphosphane;nitrate;Bis(triphenylphosphine)copper(1+) nitrate;23751-62-4;DTXSID20558957;MFCD02091690;bis(triphenylphosphine)copper(i)nitrate;F82205;Copper(1+) nitrate--triphenylphosphane (1/1/2)

Chemical Property of Bis(triphenylphosphine)copper(I) nitrate

Chemical Property:

• PSA: 96.06000
• LogP: 7.17120
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 6
• Exact Mass: 649.099690
• Heavy Atom Count: 43
• Complexity: 220

Purity/Quality:

98%,99%, ^*data from raw suppliers

Bis(triphenylphosphine)copper(I) nitrate, 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)P(C2=CC=CC=C2)C3=CC=CC=C3.C1=CC=C(C=C1)P(C2=CC=CC=C2)C3=CC=CC=C3.[N+](=O)([O-])[O-].[Cu+]

Technology Process of Bis(triphenylphosphine)copper(I) nitrate

There total 3 articles about Bis(triphenylphosphine)copper(I) nitrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

copper(II) nitrate trihydrate + triphenylphosphine (603-35-0) → bis(triphenylphosphino)copper(I) nitrate (14494-93-0,23751-62-4,106678-35-7)

Guidance literature:

In ethanol; for 0.833333h; Schlenk technique; Reflux; Inert atmosphere;

Reference yield: 62.0%

copper(II) nitrate + triphenylphosphine (603-35-0) → bis(triphenylphosphino)copper(I) nitrate (14494-93-0,23751-62-4,106678-35-7)

Guidance literature:

In methanol; water; for 0.5h; Heating / reflux;

Reference yield:

copper(II) nitrate dihydrate + triphenylphosphine (603-35-0) → bis(triphenylphosphino)copper(I) nitrate (14494-93-0,23751-62-4,106678-35-7)

Guidance literature:

In methanol; for 0.166667h; Reflux;

DOI:10.14233/ajchem.2020.22432

upstream raw materials:

triphenylphosphine

Downstream raw materials:

[Cu(PPh₃)2(4-amino-1,2,4-triazin-3(2H)-thione-5-one)]NO₃

(3-hydroxy-3-(p-methylphenyl)-2-propenedithioate-S,S')bis(triphenylphosphine-P)copper(I)

(3-hydroxy-3-(p-fluorophenyl)-2-propenedithioate-S,S')bis(triphenylphosphine-P)copper(I)

(3-hydroxy-3-(p-chlorophenyl)-2-propenedithioate-S,S')bis(triphenylphosphine-P)copper(I)

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