N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

Base Information

Chemical Name:N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide
CAS No.:1427549-80-1
Molecular Formula:C₂₈H₁₉BrClN₃O₅
Molecular Weight:592.833
Hs Code.:

Synonyms:N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

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Chemical Property of N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

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Technology Process of N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

There total 5 articles about N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 1427549-70-9
C₁₈H₁₆BrN₃O₃

: 1427549-80-1
N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

Guidance literature:: With sodium carbonate; In dimethyl sulfoxide; at 20 ℃; for 24h;
DOI:10.3390/molecules171214434

Reference yield:

: 91891-24-6
N-(3-hydroxyphenyl)-2-oxopyrrolidine-4-carboxylic acid

: 1427549-80-1
N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 5 h / Reflux

2: hydrazine hydrate / isopropyl alcohol / 5 h / Reflux

3: isopropyl alcohol / 3 h / Reflux

4: sodium carbonate / dimethyl sulfoxide / 24 h / 20 °C

With sulfuric acid; sodium carbonate; hydrazine hydrate; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.3390/molecules171214434

Reference yield:

: 105041-77-8
1-(3-hydroxyphenyl)-5-oxo-3-pyrrolidinecarbohydrazide

: 1427549-80-1
N'-[(4-bromophenyl)methylidene]-1-{3-[(3-chloro-1,4-dioxo-1,4-dihydro-2-naphthalenyl)oxy]phenyl}-5-oxo-3-pyrrolidinecarbohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: isopropyl alcohol / 3 h / Reflux

2: sodium carbonate / dimethyl sulfoxide / 24 h / 20 °C

With sodium carbonate; In dimethyl sulfoxide; isopropyl alcohol;
DOI:10.3390/molecules171214434