(2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

Base Information

Chemical Name:(2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate
CAS No.:1400745-10-9
Molecular Formula:C₄₃H₆₂Cl₂N₂O₄
Molecular Weight:741.882
Hs Code.:

Synonyms:(2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

Suppliers and Price of (2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of (2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

There total 2 articles about (2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.5%

: 1400745-80-3
(2-(piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

: 50-30-6
2,6-dichlorobenzoic acid

: 1400745-10-9
(2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; at 20 ℃;
DOI:10.1016/j.ejmech.2012.08.048

Reference yield:

: 1208130-73-7
2-bromoethyl 3β-hydroxyurs-12-en-28-oate

: 1400745-10-9
(2-(4-(2,6-dichlorobenzoyl)piperazin-1-yl)ethyl) 3-hydroxy-urs-12-en-28-oate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 0.17 h / 20 °C

1.2: 5 h / 80 °C

2.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; triethylamine / dichloromethane / 20 °C

With potassium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2012.08.048