C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

Base Information

Chemical Name:C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S
CAS No.:1180011-69-1
Molecular Formula:C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S
Molecular Weight:637.508
Hs Code.:

C<sub>2</sub>HF<sub>3</sub>O<sub>2</sub>*C<sub>20</sub>H<sub>22</sub>F<sub>5</sub>N<sub>5</sub>O<sub>4</sub>S

Synonyms:C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

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Chemical Property of C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

Chemical Property:

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Technology Process of C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

There total 13 articles about C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1178584-06-9
N-[3-(2-bromoacetyl)-5-(pentafluorosulfanyl)phenyl]acetamide

: 1180011-85-1
2,3-diethoxyimidazo[1,5-b]pyridazin-7-ylamine trifluoroacetate

: 76-05-1
trifluoroacetic acid

: 1180011-69-1
C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

Guidance literature:: N-[3-(2-bromoacetyl)-5-(pentafluorosulfanyl)phenyl]acetamide; 2,3-diethoxyimidazo[1,5-b]pyridazin-7-ylamine trifluoroacetate; With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide;

trifluoroacetic acid; In water; acetonitrile;

Reference yield:

: 833-96-5
3-(pentafluoro-λ⁶-sulphanyl)benzoic acid

: 1180011-69-1
C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

Guidance literature:: Multi-step reaction with 8 steps

1.1: nitric acid / 20 °C

1.2: 75 °C

2.1: thionyl chloride / Reflux

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

4.1: hydrogen / Raney nickel / methanol / 5 h

5.1: triethylamine / dichloromethane / 3 h / 20 °C

6.1: lithium hexamethyldisilazane / tert-butyl methyl ether; tetrahydrofuran / 0.5 h / 0 °C

6.2: 2.5 h / 0 - 20 °C

6.3: Cooling with ice

7.1: phenyltrimethylammonium tribromide / tetrahydrofuran; methanol / 5 h / 20 - 40 °C

8.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With thionyl chloride; hydrogen; nitric acid; phenyltrimethylammonium tribromide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; Raney nickel; In tetrahydrofuran; methanol; dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide;

Reference yield:

: 852469-45-5
3-nitro-5-(pentafluoro-λ⁶-sulfanyl)benzoic acid

: 1180011-69-1
C₂HF₃O₂*C₂₀H₂₂F₅N₅O₄S

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride / Reflux

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

3.1: hydrogen / Raney nickel / methanol / 5 h

4.1: triethylamine / dichloromethane / 3 h / 20 °C

5.1: lithium hexamethyldisilazane / tert-butyl methyl ether; tetrahydrofuran / 0.5 h / 0 °C

5.2: 2.5 h / 0 - 20 °C

5.3: Cooling with ice

6.1: phenyltrimethylammonium tribromide / tetrahydrofuran; methanol / 5 h / 20 - 40 °C

7.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide

With thionyl chloride; hydrogen; phenyltrimethylammonium tribromide; triethylamine; N-ethyl-N,N-diisopropylamine; lithium hexamethyldisilazane; Raney nickel; In tetrahydrofuran; methanol; dichloromethane; tert-butyl methyl ether; N,N-dimethyl-formamide;