1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

Base Information

Chemical Name:1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine
CAS No.:1360871-87-9
Molecular Formula:C₁₈H₁₇Cl₃N₂
Molecular Weight:367.705
Hs Code.:

Synonyms:1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

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Chemical Property of 1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

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Technology Process of 1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

There total 5 articles about 1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1360871-90-4
N-(4-chlorobenzoyl)-N'-(3,4-dichlorophenyl)pentamethylenediamine

: 1360871-87-9
1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

Guidance literature:: N-(4-chlorobenzoyl)-N'-(3,4-dichlorophenyl)pentamethylenediamine; In chloroform; at 70 ℃; for 0.116667h; Microwave irradiation;

With sodium hydroxide; In water; at -5 ℃; pH=14;
DOI:10.1016/j.tetlet.2012.01.009

Reference yield:

: 1245641-13-7
N-(3,4-dichlorophenyl)pentamethylenediamine

: 1360871-87-9
1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / -10 - 20 °C

2.1: ethyl polyphosphate / chloroform / 0.12 h / 70 °C / Microwave irradiation

2.2: -5 °C / pH 14

With triethylamine; In dichloromethane; chloroform;
DOI:10.1016/j.tetlet.2012.01.009

Reference yield:

: 1204415-01-9
C₁₂H₁₅Cl₂NO

: 1360871-87-9
1-(3,4-dichlorophenyl)-2-(4-chlorophenyl)-1,4,5,6,7,8-hexahydro-1,3-diazocine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 100 °C / Neat (no solvent)

2.1: ethyl polyphosphate / chloroform / 0.12 h / 70 °C / Microwave irradiation

2.2: -5 °C / pH 14

With ethyl polyphosphate; In chloroform;
DOI:10.1016/j.tetlet.2012.01.009