trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone

Base Information

Chemical Name:trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone
CAS No.:138212-44-9
Molecular Formula:C₁₆H₂₁NO₄S
Molecular Weight:323.413
Hs Code.:

Synonyms:trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone

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Chemical Property of trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone

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Technology Process of trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone

There total 7 articles about trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 122053-44-5
(Z)-2,2-dimethylhex-4-en-3-ol

: 4083-64-1
Tosyl isocyanate

: 138212-44-9
trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone

Guidance literature:: (Z)-2,2-dimethylhex-4-en-3-ol; Tosyl isocyanate; In tetrahydrofuran; at 20 ℃; for 1h; Schlenk technique;

With sodium acetate; palladium diacetate; acetic acid; p-benzoquinone; In tetrahydrofuran; dimethyl sulfoxide; at 50 ℃; for 48h; diastereoselective reaction; Schlenk technique;
DOI:10.1002/chem.201202359

Reference yield: 53.0%

: 131141-50-9
O-(1-tert-butyl-2,3-butadienyl) N-tosylcarbamate

: 138212-44-9
trans-N-p-toluenesulfonyl-5-t-butyl-4-vinyl-2-oxazolidinone

Guidance literature:: With triethylamine; silver trifluoromethanesulfonate; In benzene; 1.) 50 deg C, 21 h, 2.) reflux, 20 h;
DOI:10.1016/0040-4039(91)80169-7