N¹-(3-Cyanphenyl)-N²-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid

Base Information

• Chemical Name: N¹-(3-Cyanphenyl)-N²-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid
• CAS No.: 130296-43-4
• Molecular Formula: C₄₅H₃₃N₃O₄
• Molecular Weight: 679.775

Synonyms:N¹-(3-Cyanphenyl)-N²-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid

Chemical Property of N¹-(3-Cyanphenyl)-N²-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid

Chemical Property:

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Technology Process of N¹-(3-Cyanphenyl)-N²-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid

There total 4 articles about N¹-(3-Cyanphenyl)-N²-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

N2-(2,5-Di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid (130296-50-3) + m-cyanoaniline (2237-30-1) → N1-(3-Cyanphenyl)-N2-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid (130296-43-4)

Guidance literature:

With zinc diacetate; In quinoline; at 220 ℃; for 3h;

Reference yield:

perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-carboxamide (33955-42-9) → N1-(3-Cyanphenyl)-N2-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid (130296-43-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / Zn(OAc)2 / quinoline / 2 h / 220 °C

2: 63 percent / Zn(OAc)2 / quinoline / 3 h / 220 °C

With zinc diacetate; In quinoline;

Reference yield:

2,5-di-tert-butylaniline (21860-03-7) → N1-(3-Cyanphenyl)-N2-(2,5-di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid (130296-43-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 88 percent / Zn(OAc)2 / quinoline / 2 h / 220 °C

2: 63 percent / Zn(OAc)2 / quinoline / 3 h / 220 °C

With zinc diacetate; In quinoline;

upstream raw materials:

N²-(2,5-Di-tert-butylphenyl)-3,4:9,10-perylentetracarboxdiimid

m-cyanoaniline

perylene-3,4,9,10-tetracarboxylic-3,4-anhydride-9,10-carboxamide

2,5-di-tert-butylaniline

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