Cyclohexanone, 5-methyl-2-(1-methylethylidene)-, oxime, [R-(Z)]- (9CI)

Base Information

• Chemical Name: Cyclohexanone, 5-methyl-2-(1-methylethylidene)-, oxime, [R-(Z)]- (9CI)
• CAS No.: 106550-19-0
• Molecular Formula: C₁₀H₁₇NO
• Molecular Weight: 167.251
• Mol file: 106550-19-0.mol

Synonyms:Cyclohexanone, 5-methyl-2-(1-methylethylidene)-, oxime, [R-(Z)]- (9CI)

Chemical Property of Cyclohexanone, 5-methyl-2-(1-methylethylidene)-, oxime, [R-(Z)]- (9CI)

Chemical Property:

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Technology Process of Cyclohexanone, 5-methyl-2-(1-methylethylidene)-, oxime, [R-(Z)]- (9CI)

There total 2 articles about Cyclohexanone, 5-methyl-2-(1-methylethylidene)-, oxime, [R-(Z)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(+)-pulegone (89-82-7,90449-51-7) → oxime Z de la methyl-5 (methyl-1 ethylidene)-2 cyclohexanone (57291-09-5,106550-02-1,106550-19-0,321359-55-1) + oxime E de la methyl-5 (methyl-1 ethylidene)-2 cyclohexanone (57291-09-5,106550-02-1,106550-19-0,321359-55-1)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 2h; Yield given. Yields of byproduct given; Heating;

Reference yield:

(+)-pulegone (89-82-7,90449-51-7) → oxime Z de la methyl-5 (methyl-1 ethylidene)-2 cyclohexanone (57291-09-5,106550-02-1,106550-19-0,321359-55-1) + oxime E de la methyl-5 (methyl-1 ethylidene)-2 cyclohexanone (57291-09-5,106550-02-1,106550-19-0,321359-55-1)

Guidance literature:

With hydroxylamine hydrochloride; In ethanol; for 2h; Yield given. Yields of byproduct given; Heating;

Reference yield: 10.0%

phenylmagnesium bromide + oxime Z de la methyl-5 (methyl-1 ethylidene)-2 cyclohexanone (57291-09-5,106550-02-1,106550-19-0,321359-55-1) → methyl-5 (methyl-1 ethenyl)-2 phenyl-1 aza-7 bicyclo<4,1,0>heptane (106550-07-6)

Guidance literature:

In toluene; for 20h; Heating;

upstream raw materials:

(+)-pulegone

Downstream raw materials:

methyl-5 (methyl-1 ethenyl)-2 phenyl-1 aza-7 bicyclo<4,1,0>heptane

((1R,5R,6R)-2-Isopropenyl-5-methyl-1-phenyl-7-aza-bicyclo[4.1.0]hept-7-yl)-(4-nitro-phenyl)-methanone

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