(E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

Base Information

Chemical Name:(E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate
CAS No.:1227625-50-4
Molecular Formula:C₄₄H₆₃NO₅
Molecular Weight:685.988
Hs Code.:

Synonyms:(E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

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Chemical Property of (E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

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Technology Process of (E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

There total 7 articles about (E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 111772-62-4
2-hydroxy-4-n-dodecyloxybenzaldehyde

: 163855-99-0
4-(dodecyloxy)phenyl 4-aminobenzoate

: 1227625-50-4
(E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; for 5h; Reflux;
DOI:10.1071/CH09405

Reference yield:

: 143-15-7
1-dodecylbromide

: 1227625-50-4
(E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / butan-1-ol / 0.5 h / 20 °C / Inert atmosphere

1.2: 60 h / 100 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 13 h / 0 - 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 24 h / 20 °C

4.1: toluene-4-sulfonic acid / ethanol / 5 h / Reflux

With dmap; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1071/CH09405

Reference yield:

: 123-31-9,8027-02-9
hydroquinone

: 1227625-50-4
(E)-4-(dodecyloxy)phenyl 4-(4-(dodecyloxy)-2-hydroxybenzylideneamino)benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydroxide / butan-1-ol / 0.5 h / 20 °C / Inert atmosphere

1.2: 60 h / 100 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 13 h / 0 - 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / tetrahydrofuran; ethanol / 24 h / 20 °C

4.1: toluene-4-sulfonic acid / ethanol / 5 h / Reflux

With dmap; palladium 10% on activated carbon; hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; butan-1-ol;
DOI:10.1071/CH09405