N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

Base Information

Chemical Name:N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline
CAS No.:672306-05-7
Molecular Formula:C₂₉H₄₉NO₄
Molecular Weight:475.712
Hs Code.:

Synonyms:N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

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Chemical Property of N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

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Technology Process of N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

There total 4 articles about N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 619261-14-2
N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undec-8-en-9-yl)aniline

: 672306-05-7
N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

Guidance literature:: With hydrogen; 10percent Pd/C; In tetrahydrofuran; ethanol; for 48h; under 760.051 Torr;
DOI:10.1002/ejoc.200200693

Reference yield:

: 17229-11-7
2-(2-chloroethoxy)-2-methylpropane

: 672306-05-7
N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

Guidance literature:: Multi-step reaction with 4 steps

1.1: 66 percent / K₂CO₃; KI / butan-1-ol / Heating

2.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / -78 °C

2.2: hexane; tetrahydrofuran / -60 - 20 °C

3.1: p-toluenesulfonic acid monohydrate / toluene / Heating

4.1: 66 percent / H₂ / 10percent Pd/C / tetrahydrofuran; ethanol / 48 h / 760.05 Torr

With n-butyllithium; hydrogen; potassium carbonate; toluene-4-sulfonic acid; potassium iodide; 10percent Pd/C; In tetrahydrofuran; ethanol; hexane; toluene; butan-1-ol;
DOI:10.1002/ejoc.200200693

Reference yield:

: 681028-85-3
4-bromo-N,N-bis(2-tert-butoxyethyl)aniline

: 672306-05-7
N,N-bis(2-tert-butoxyethyl)-4-(3,3-dimethyl-1,5-dioxaspiro[5.5]undecan-9-yl)aniline

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / 2 h / -78 °C

1.2: hexane; tetrahydrofuran / -60 - 20 °C

2.1: p-toluenesulfonic acid monohydrate / toluene / Heating

3.1: 66 percent / H₂ / 10percent Pd/C / tetrahydrofuran; ethanol / 48 h / 760.05 Torr

With n-butyllithium; hydrogen; toluene-4-sulfonic acid; 10percent Pd/C; In tetrahydrofuran; ethanol; hexane; toluene;
DOI:10.1002/ejoc.200200693