trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester
CAS No.:917379-65-8
Molecular Formula:C₂₁H₁₅F₂₉O₃S
Molecular Weight:898.368
Hs Code.:

Synonyms:trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

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Chemical Property of trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

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Technology Process of trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

There total 5 articles about trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 917379-64-7
6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluorononyl)undecan-1-ol

: 358-23-6
trifluoromethylsulfonic anhydride

: 917379-65-8
trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; at -15 - 20 ℃;
DOI:10.1016/j.jfluchem.2005.12.031

Reference yield:

: 917379-63-6
6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecanoic acid

: 917379-65-8
trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / borane*THF complex / tetrahydrofuran / 16 h / Heating

2: 97 percent / pyridine / dimethylformamide / -15 - 20 °C

With pyridine; borane-THF; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2005.12.031

Reference yield:

: 917379-61-4
2,2-bis-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-malonic acid

: 917379-65-8
trifluoro-methanesulfonic acid 6,6,7,7,8,8,9,9,10,10,11,11,11-tridecafluoro-2-(4,4,5,5,6,6,7,7,8,8,9,9,9-tridecafluoro-nonyl)-undecyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / 0.75 h / 190 °C

2: 97 percent / borane*THF complex / tetrahydrofuran / 16 h / Heating

3: 97 percent / pyridine / dimethylformamide / -15 - 20 °C

With pyridine; borane-THF; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1016/j.jfluchem.2005.12.031