C₁₆H₂₄BrNO₃S₂

Base Information

• Chemical Name: C₁₆H₂₄BrNO₃S₂
• CAS No.: 1383917-32-5
• Molecular Formula: C₁₆H₂₄BrNO₃S₂
• Molecular Weight: 422.407
• Mol file: 1383917-32-5.mol

Synonyms:C₁₆H₂₄BrNO₃S₂

Chemical Property of C₁₆H₂₄BrNO₃S₂

Chemical Property:

Purity/Quality:

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Technology Process of C₁₆H₂₄BrNO₃S₂

There total 9 articles about C₁₆H₂₄BrNO₃S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

C16H23NO3S2 → C16H24BrNO3S2 (1383917-32-5)

Guidance literature:

With N-Bromosuccinimide; sodium cyanoborohydride;

Reference yield: 61.0%

deca-3,4-dien-1-yl sulfamate (1284257-82-4) + thiophenol (108-98-5) → C16H24BrNO3S2 (1383917-32-5)

Guidance literature:

deca-3,4-dien-1-yl sulfamate; thiophenol; With dirhodium(II) tetrakis(triphenylacetate); iodosylbenzene; In dichloromethane; at 20 ℃; for 1h;

With N-Bromosuccinimide; sodium cyanoborohydride; In dichloromethane; at 0 ℃; for 0.166667h;

Reference yield:

C16H22BrNO3S2 → C16H24BrNO3S2 (1383917-32-5)

Guidance literature:

With sodium cyanoborohydride; In tetrahydrofuran; methanol; acetic acid; at 0 - 20 ℃; for 1h; optical yield given as %de; diastereoselective reaction;

DOI:10.1021/ja304859w

upstream raw materials:

(R)-(-)-deca-3,4-dien-1-ol

C₁₀H₁₉NO₃S

1-octyn-3-ol

deca-3,4-dien-1-yl sulfamate