(2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

Base Information

Chemical Name:(2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester
CAS No.:852997-10-5
Molecular Formula:C₁₆H₁₇BrF₃NO₂
Molecular Weight:392.216
Hs Code.:

Synonyms:(2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

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Chemical Property of (2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

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Technology Process of (2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

There total 1 articles about (2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 513-31-5
2-bromoallyl bromide

: 509093-24-7
4-(benzyloxycarbonyl)amino-5,5,5-trifluoropent-1-ene

: 852997-10-5
(2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

Guidance literature:: With tetra-(n-butyl)ammonium iodide; sodium hydride; In N,N-dimethyl-formamide; at 90 ℃; for 24h;
DOI:10.1055/s-2005-864812

Reference yield: 27.0%

: 852997-10-5
(2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

: 624-48-6
dimethyl cis-but-2-ene-1,4-dioate

: 3-trifluoromethyl-3,4,5,6,7,8-hexahydro-1H-isoquinoline-2,6,7-tricarboxylic acid 2-benzyl ester 6,7-dimethyl ester

Guidance literature:: (2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester; With triphenylphosphine; silver carbonate; palladium diacetate; In acetonitrile; at 90 ℃; for 6h;

dimethyl cis-but-2-ene-1,4-dioate; In acetonitrile; at 90 ℃; for 18h;
DOI:10.1055/s-2005-864812

Reference yield: 17.0%

: 852997-10-5
(2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 3-trifluoromethyl-3,4,5,6,7,8-hexahydro-1H-isoquinoline-2,6-dicarboxylic acid 2-benzyl ester 6-methyl ester

Guidance literature:: (2-bromo-allyl)-(1-trifluoromethyl-but-3-enyl)-carbamic acid benzyl ester; With triphenylphosphine; silver carbonate; palladium diacetate; In acetonitrile; at 90 ℃; for 6h;

acrylic acid methyl ester; In acetonitrile; at 90 ℃; for 18h;
DOI:10.1055/s-2005-864812