allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

Base Information

Chemical Name:allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate
CAS No.:524071-48-5
Molecular Formula:C₃₇H₃₇N₂O₅P
Molecular Weight:620.685
Hs Code.:

Synonyms:allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

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Chemical Property of allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

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Technology Process of allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

There total 1 articles about allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 524071-47-4
allyl [(2R,3S)-2-[2-(3-{[(tert-butoxycabonyl)-amino]-methyl}-phenyl)-2-oxoethyl]-3-((1R)-1-{[tert-butyl-(dimethyl)-silyl]-oxy}-ethyl)-4-oxoazetidin-1-yl] (triphenylphosphoranilidene) acetate

: 524071-48-5
allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

Guidance literature:: With trifluoroacetic acid; In water; at 20 ℃; for 1h;

Reference yield:

: 524071-48-5
allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate

: 5819-21-6
4-nitrophenyl N-methylcarbamate

: 2937-50-0
Allyl chloroformate

: 524071-49-6
allyl ((2R,3S)-3-((1R)-1-{[(allyloxy)-carbonyl]-oxy}-ethyl)-2-{2-[3-({[(methylamino)-carbonyl]-amino}-methyl)-phenyl]-2-oxoethyl}-4-oxoazetidin-1-yl) (triphenylphosphoranilidene) acetate

Guidance literature:: allyl {(2R,3S)-2-{2-[3-(aminomethyl)-phenyl]-2-oxoethyl}-3-[(1R)-1-hydroxyethyl]-4-oxoazetidin-1-yl} (triphenylphosphoranilidene) acetate; 4-nitrophenyl N-methylcarbamate; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; for 2h;

Allyl chloroformate; With dmap; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 14h;