3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

Base Information

Chemical Name:3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone
CAS No.:142852-08-2
Molecular Formula:C₂₃H₂₈N₂O
Molecular Weight:348.488
Hs Code.:

Synonyms:3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

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Chemical Property of 3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

Chemical Property:

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Technology Process of 3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

There total 4 articles about 3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16078-30-1
1-Acetyl-2,3-dihydro-1H-indole

: 142852-08-2
3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / 1,2-dichloro-ethane / 12 h / 65 - 70 °C

2: conc. HCl / 16 h / Heating

3: K₂CO₃ / ethanol / 3 h / Ambient temperature

With hydrogenchloride; aluminium trichloride; potassium carbonate; In ethanol; 1,2-dichloro-ethane;
DOI:10.1021/jm00041a007

Reference yield:

: 142853-09-6
3-(1-acetyl-4-piperidinyl)propionyl chloride

: 142852-08-2
3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

Guidance literature:: Multi-step reaction with 3 steps

1: AlCl₃ / 1,2-dichloro-ethane / 12 h / 65 - 70 °C

2: conc. HCl / 16 h / Heating

3: K₂CO₃ / ethanol / 3 h / Ambient temperature

With hydrogenchloride; aluminium trichloride; potassium carbonate; In ethanol; 1,2-dichloro-ethane;
DOI:10.1021/jm00041a007

Reference yield:

: 142853-10-9
1-Acetyl-5-[3-(1-acetylpiperidin-4-yl)-1-oxopropyl]-2,3-dihydro-1H-indole

: 142852-08-2
3-[1-(phenylmethyl)-4-piperidinyl)-1-(2,3-dihydroindole-5-yl)-1-propanone

Guidance literature:: Multi-step reaction with 2 steps

1: conc. HCl / 16 h / Heating

2: K₂CO₃ / ethanol / 3 h / Ambient temperature

With hydrogenchloride; potassium carbonate; In ethanol;
DOI:10.1021/jm00041a007