(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

Base Information

Chemical Name:(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)
CAS No.:1005520-00-2
Molecular Formula:C₃₆H₇₂OSeSi₇
Molecular Weight:796.526
Hs Code.:

Synonyms:(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

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Chemical Property of (2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

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Technology Process of (2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

There total 2 articles about (2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: (Z)-1,2-dimesityl-1,2-bis{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}disilene

: 1005520-00-2
(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

Guidance literature:: (Z)-1,2-dimesityl-1,2-bis{2,4,6-tris[bis(trimethylsilyl)methyl]phenyl}disilene; In tetrahydrofuran; at 60 ℃; for 20h;

With water; In tetrahydrofuran; benzene; Further stages.;
DOI:10.1002/ejic.200601226

Reference yield: 62.0%

: 185910-18-3
1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene

: 1005520-00-2
(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

Guidance literature:: 1,2-bis(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)-1,2-bis(2,4,6-trimethylphenyl)-disilene; With Bis(η-cyclopentadienyl)(pentaselenido)zirconium; In tetrahydrofuran; at 60 ℃; for 20h; Inert atmosphere;

In benzene;
DOI:10.1016/j.jorganchem.2008.11.001

Reference yield: 90.0%

: 1005520-00-2
(2,4,6-tris(bis(trimethylsilyl)methyl)phenyl)(2,4,6-trimethylphenyl)Si(SeH)(OH)

: 10199-34-5,14056-88-3,15604-36-1
cis-dichlorobis(triphenylphosphine)platinum(II)

: 1025455-44-0
[(2,4,6-tris[bis(trimethylsilyl)methyl]phenyl)(mesityl)Si(μ-O)(μ-Se)Pt(triphenylphosphine)2]

Guidance literature:: With sodium hydride; In tetrahydrofuran; treatment of (C6H2(CH(SiMe3)2)3)(Mes)Si(OH)(SeH) with 2 molar equiv. of NaH at 0°C; addn. of THF soln. of cis-PtCl2(PPh3)2 at 0°C;warming to room temp.;
DOI:10.1021/om800210g