3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride

Base Information

• Chemical Name: 3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride
• CAS No.: 1192189-50-6
• Molecular Formula: C₂₂H₂₇N₃O₃*ClH
• Molecular Weight: 417.936

Synonyms:3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride

Chemical Property of 3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride

Chemical Property:

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Technology Process of 3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride

There total 1 articles about 3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyl 4-benzyl-4-(3-(dimethylcarbamoyloxy)-phenylcarbamoyl)piperidine-1-carboxylate (1192189-49-3) → 3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride (1192189-50-6)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; methanol; at 50 ℃; for 1h;

Reference yield: 81.0%

3-(4-benzylpiperidine-4-carboxamido)phenyl dimethylcarbamate hydrochloride (1192189-50-6) + 4-chloro-5-methyl-7H-pyrrolo[2,3-d]pyrimidine (1618-36-6) → 3-(4-benzyl-1-(5-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidine-4-carboxamido)phenyl dimethylcarbamate (1192189-48-2)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In isopropyl alcohol; at 120 ℃;

upstream raw materials:

tert-butyl 4-benzyl-4-(3-(dimethylcarbamoyloxy)-phenylcarbamoyl)piperidine-1-carboxylate

Downstream raw materials:

3-(4-benzyl-1-(5-methyl-7H-pyrrolo[2,3-d]pyrimidin-4-yl)piperidine-4-carboxamido)phenyl dimethylcarbamate

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