N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

Base Information

• Chemical Name: N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide
• CAS No.: 1124353-60-1
• Molecular Formula: C₄₅H₄₃N₅O₄
• Molecular Weight: 717.868

Synonyms:N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

Chemical Property of N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

Chemical Property:

Purity/Quality:

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Technology Process of N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

There total 1 articles about N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N-(4-bromomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-59-8) → N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-60-1)

Guidance literature:

With sodium azide; In N,N-dimethyl-formamide; at 80 ℃; for 2h;

DOI:10.1002/ejoc.200800805

Reference yield: 75.0%

N,N-Dimethylpropargylamin (7223-38-3) + N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-60-1) → N-4-(4-dimethylaminomethyl[1,2,3]triazol-1-ylmethyl)benzyl-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-63-4) + N-4-(4-dimethylaminomethyl-5-iodo[1,2,3]triazol-1-ylmethyl)benzyl-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-74-7)

Guidance literature:

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1002/ejoc.200800805

Reference yield: 73.0%

N-(4-azidomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-60-1) + Pargyline (555-57-7) → N-4-{4-[(benzyl(methyl)amino)methyl][1,2,3]triazol-1-ylmethyl}benzyl-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide (1124353-64-5)

Guidance literature:

With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1002/ejoc.200800805

upstream raw materials:

N-(4-bromomethylbenzyl)-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

Downstream raw materials:

N-4-(4-dimethylaminomethyl[1,2,3]triazol-1-ylmethyl)benzyl-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

N-4-(4-dimethylaminomethyl-5-iodo[1,2,3]triazol-1-ylmethyl)benzyl-N'-(1-hexylheptyl)perylene-3,4:9,10-tetracarboxdiimide

N-(1-hexylheptyl)-N'-4-(4-propyl[1,2,3]triazol-1-ylmethyl)benzylperylene-3,4:9,10-tetracarboxdiimide

N-(1-hexylheptyl)-N'-4-(5-iodol-4-propyl[1,2,3]triazol-1-ylmethyl)benzylperylene-3,4:9,10-tetracarboxdiimide

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