8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

Base Information

Chemical Name:8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol
CAS No.:102104-35-8
Molecular Formula:C₁₈H₂₅ClO₄S
Molecular Weight:372.913
Hs Code.:

Synonyms:8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

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Technology Process of 8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

There total 3 articles about 8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13307-61-4
Isobutylthiobenzene

: 102104-35-8
8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

Guidance literature:: Multi-step reaction with 3 steps

1: N-chlorosuccinimide / CCl₄ / 2.5 h / Ambient temperature

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / -60 - -40 °C

3: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min

With N-chloro-succinimide; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrachloromethane; dichloromethane;
DOI:10.1246/bcsj.58.1983

Reference yield:

: 72653-48-6
α-chloroisobutyl phenyl sulfide

: 102104-35-8
8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

Guidance literature:: Multi-step reaction with 2 steps

1: m-chloroperoxybenzoic acid / CH₂Cl₂ / -60 - -40 °C

2: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min

With 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In dichloromethane;
DOI:10.1246/bcsj.58.1983

Reference yield:

: 108-98-5
thiophenol

: 102104-35-8
8-(1-Benzenesulfinyl-1-chloro-2-methyl-propyl)-1,4-dioxa-spiro[4.5]decan-8-ol

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / NaOEt / ethanol / 3 h / Ambient temperature

2: N-chlorosuccinimide / CCl₄ / 2.5 h / Ambient temperature

3: m-chloroperoxybenzoic acid / CH₂Cl₂ / -60 - -40 °C

4: 1) lithium diisopropylamide / 1) THF, -70 deg C, 20 min, 2) THF, -70 deg C, 10 min

With N-chloro-succinimide; sodium ethanolate; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrachloromethane; ethanol; dichloromethane;
DOI:10.1246/bcsj.58.1983