4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Base Information

Chemical Name:4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester
CAS No.:1448311-89-4
Molecular Formula:C₁₆H₂₃ClO₃
Molecular Weight:298.81
Hs Code.:

Synonyms:4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Suppliers and Price of 4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

There total 8 articles about 4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 76811-97-7
4-(4-chloro-1-oxobutyl)-α,α-dimethylbenzeneacetic acid ethyl ester

: 1448311-89-4
4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Guidance literature:: With sodium tetrahydroborate; In ethanol; at 25 - 30 ℃; for 7h;
DOI:10.1007/s11164-012-0747-y

Reference yield:

: 18755-52-7
(2-acetoxy-1,1-dimethylethyl)benzene

: 1448311-89-4
4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: aluminum (III) chloride / dichloromethane / 2.33 h / -5 - 0 °C

1.2: 5 h / 0 °C

2.1: methanol; sodium hydroxide / 4 h / 25 - 30 °C

3.1: water; acetic acid; potassium permanganate / acetone / 7 h / 25 - 45 °C

4.1: hydrogenchloride / 7 h / 40 - 45 °C

5.1: sodium tetrahydroborate / ethanol / 7 h / 25 - 30 °C

With hydrogenchloride; methanol; aluminum (III) chloride; sodium tetrahydroborate; potassium permanganate; water; acetic acid; sodium hydroxide; In ethanol; dichloromethane; acetone;
DOI:10.1007/s11164-012-0747-y

Reference yield:

: 169032-11-5
2-(4-(4-Chloro-1-oxo-butyl))-phenyl-2-methyl propanyl acetate

: 1448311-89-4
4-(4-chloro-1-hydroxyl-butyl)-α,α-dimethyl phenyl acetic acid ethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: methanol; sodium hydroxide / 4 h / 25 - 30 °C

2: water; acetic acid; potassium permanganate / acetone / 7 h / 25 - 45 °C

3: hydrogenchloride / 7 h / 40 - 45 °C

4: sodium tetrahydroborate / ethanol / 7 h / 25 - 30 °C

With hydrogenchloride; methanol; sodium tetrahydroborate; potassium permanganate; water; acetic acid; sodium hydroxide; In ethanol; acetone;
DOI:10.1007/s11164-012-0747-y