Cyclohexanecarboxylic acid, 1-methyl-2-nitro-, methyl ester, trans- (9CI)

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 1-methyl-2-nitro-, methyl ester, trans- (9CI)
CAS No.:106334-36-5
Molecular Formula:C₉H₁₅NO₄
Molecular Weight:201.222
Hs Code.:
Mol file:106334-36-5.mol

Synonyms:Cyclohexanecarboxylic acid, 1-methyl-2-nitro-, methyl ester, trans- (9CI)

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Chemical Property of Cyclohexanecarboxylic acid, 1-methyl-2-nitro-, methyl ester, trans- (9CI)

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Technology Process of Cyclohexanecarboxylic acid, 1-methyl-2-nitro-, methyl ester, trans- (9CI)

There total 4 articles about Cyclohexanecarboxylic acid, 1-methyl-2-nitro-, methyl ester, trans- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 106334-27-4
2-(2-nitropropyl)-1,3-dioxolane

: 106334-34-3,106334-35-4
2-Bromo-1-methyl-2-nitro-cyclohexanecarboxylic acid methyl ester

: 106334-36-5,106334-37-6
2-methyl-2-carbomethoxynitrocyclohexane

: 106334-38-7,106334-39-8
C₁₂H₂₀N₂O₈

Guidance literature:: With lithium methanolate; In dimethyl sulfoxide; for 24h;
DOI:10.1016/S0040-4020(01)87381-6

Reference yield:

: 106334-34-3,106334-35-4
2-Bromo-1-methyl-2-nitro-cyclohexanecarboxylic acid methyl ester

: 106334-36-5,106334-37-6
2-methyl-2-carbomethoxynitrocyclohexane

Guidance literature:: With sodium tetrahydroborate; In methanol; water; at 20 ℃; for 26h; Yield given;
DOI:10.1016/S0040-4020(01)87381-6

Reference yield:

: 106334-33-2
2-methyl-2-carbomethoxycyclohexanone oxime

: 106334-36-5,106334-37-6
2-methyl-2-carbomethoxynitrocyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N-bromosuccinimide, sodium bicarbonate / 1.) water, 5 deg C, 2.) dioxan, 17 h

2: conc. nitric acid / pentane / 2.) room temp., 18 h

3: 21 percent / lithium methoxide / dimethylsulfoxide / 24 h

With N-Bromosuccinimide; lithium methanolate; nitric acid; sodium hydrogencarbonate; In dimethyl sulfoxide; pentane;
DOI:10.1016/S0040-4020(01)87381-6