tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

Base Information

Chemical Name:tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate
CAS No.:956235-29-3
Molecular Formula:C₃₉H₅₁N₃O₇
Molecular Weight:673.85
Hs Code.:

Synonyms:tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

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Chemical Property of tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

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Technology Process of tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

There total 9 articles about tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 956235-10-2
{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}(oxo)acetaldehyde

: 956235-28-2
tert-butyl {2-[(6-aminohexyl)oxy]ethyl}benzylcarbamate

: 956235-29-3
tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

Guidance literature:: {8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}(oxo)acetaldehyde; tert-butyl {2-[(6-aminohexyl)oxy]ethyl}benzylcarbamate; In dimethyl sulfoxide; at 20 ℃; for 5h;

With sodium tetrahydroborate; In methanol; dimethyl sulfoxide; at 0 - 20 ℃;

With ammonium chloride; In tetrahydrofuran; methanol; water; dimethyl sulfoxide;

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 956235-29-3
tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / 1,4-dioxane; water / 73 h / 5 - 20 °C

2.1: sodium hydroxide / tetrabutylammomium bromide / water / 16 h / 20 °C

3.1: N,N-dimethyl-formamide / 6 h / 75 °C

4.1: hydrazine / ethanol / 20 - 100 °C

5.1: dimethyl sulfoxide / 5 h / 20 °C

5.2: 0 - 20 °C

With sodium hydroxide; hydrazine; tetrabutylammomium bromide; In 1,4-dioxane; ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 62978-73-8
5-acetyl-8-hydroxy-2(1H)-quinolinone

: 956235-29-3
tert-butyl benzyl[2-({6-[(2-hydroxy-2-{8-[(4-methoxybenzyl)oxy]-2-oxo-1,2-dihydroquinolin-5-yl}ethyl)amino]hexyl}oxy)ethyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogencarbonate / sodium iodide / N,N-dimethyl-formamide / 40 °C

2.1: selenium(IV) oxide / 1,4-dioxane; water / Heating / reflux

3.1: dimethyl sulfoxide / 5 h / 20 °C

3.2: 0 - 20 °C

With selenium(IV) oxide; sodium hydrogencarbonate; sodium iodide; In 1,4-dioxane; water; dimethyl sulfoxide; N,N-dimethyl-formamide;