C₅₇H₆₀O₆S₃

Base Information

Chemical Name:C₅₇H₆₀O₆S₃
CAS No.:1315509-88-6
Molecular Formula:C₅₇H₆₀O₆S₃
Molecular Weight:937.298
Hs Code.:

C<sub>57</sub>H<sub>60</sub>O<sub>6</sub>S<sub>3</sub>

Synonyms:C₅₇H₆₀O₆S₃

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Chemical Property of C₅₇H₆₀O₆S₃

Chemical Property:

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Technology Process of C₅₇H₆₀O₆S₃

There total 3 articles about C₅₇H₆₀O₆S₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1315509-87-5
C₂₇H₂₁Br₃O₆S₃

: 123324-71-0
p-tert-butylphenylboronic acid

: 1315509-88-6
C₅₇H₆₀O₆S₃

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; sodium carbonate; In toluene; for 24h; Reflux;
DOI:10.1021/ol201466z

Reference yield:

: 5751-80-4
thiophene-3-carboxylic acid ethyl ester

: 1315509-88-6
C₅₇H₆₀O₆S₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / -78 - 20 °C

1.3: Reflux

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 48 h / 0 - 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; sodium carbonate / toluene / 24 h / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; sodium carbonate; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1.1: Negishi coupling reaction / 1.2: Negishi coupling reaction / 1.3: Negishi coupling reaction / 3.1: Suzuki coupling;
DOI:10.1021/ol201466z

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 1315509-88-6
C₅₇H₆₀O₆S₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C

1.2: 1 h / -78 - 20 °C

1.3: Reflux

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 48 h / 0 - 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; sodium carbonate / toluene / 24 h / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; sodium carbonate; lithium diisopropyl amide; In tetrahydrofuran; N,N-dimethyl-formamide; toluene; 1.1: Negishi coupling reaction / 1.2: Negishi coupling reaction / 1.3: Negishi coupling reaction / 3.1: Suzuki coupling;
DOI:10.1021/ol201466z