C₁₆H₁₈⁽²⁾H₄N₂O₄

Base Information

Chemical Name:C₁₆H₁₈⁽²⁾H₄N₂O₄
CAS No.:1352801-70-7
Molecular Formula:C₁₆H₂₂N₂O₄
Molecular Weight:310.33
Hs Code.:

C<sub>16</sub>H<sub>18</sub><sup>(2)</sup>H<sub>4</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₁₆H₁₈⁽²⁾H₄N₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₈⁽²⁾H₄N₂O₄

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Technology Process of C₁₆H₁₈⁽²⁾H₄N₂O₄

There total 3 articles about C₁₆H₁₈⁽²⁾H₄N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 23328-69-0
4-chloromorpholine

: N-(pivaloyloxy)benzamide-2,3,4,5,6-d₅

: 1352801-70-7
C₁₆H₁₈⁽²⁾H₄N₂O₄

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid; In methanol; at 20 ℃; for 0.25h; Inert atmosphere;
DOI:10.1021/ol203353a

Reference yield:

: 1079-02-3
benzoic acid-2,3,4,5,6-d5

: 1352801-70-7
C₁₆H₁₈⁽²⁾H₄N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 4 h / 0 - 20 °C / Inert atmosphere

2.1: sodium carbonate / water; ethyl acetate / 20 °C / Inert atmosphere

2.2: 4 h / 0 - 20 °C / Inert atmosphere

3.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid / methanol / 0.25 h / 20 °C / Inert atmosphere

With oxalyl dichloride; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; sodium carbonate; N,N-dimethyl-formamide; Trimethylacetic acid; In methanol; dichloromethane; water; ethyl acetate;
DOI:10.1021/ol203353a

Reference yield:

: 43019-90-5
benzoyl chloride-d5

: 1293990-73-4
O-pivaloylhydroxylamine trifluoromethanesulfonate salt

: 1352801-70-7
C₁₆H₁₈⁽²⁾H₄N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium carbonate / water; ethyl acetate / 20 °C / Inert atmosphere

1.2: 4 h / 0 - 20 °C / Inert atmosphere

2.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; Trimethylacetic acid / methanol / 0.25 h / 20 °C / Inert atmosphere

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; cesium acetate; sodium carbonate; Trimethylacetic acid; In methanol; water; ethyl acetate;
DOI:10.1021/ol203353a