4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

Base Information

Chemical Name:4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide
CAS No.:1116153-63-9
Molecular Formula:C₂₁H₂₅NO₂S
Molecular Weight:355.501
Hs Code.:

Synonyms:4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

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Technology Process of 4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

There total 2 articles about 4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 629-05-0
n-octyne

: 68-34-8
phenyl toluenesulfonamide

: 1116153-63-9
4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

Guidance literature:: phenyl toluenesulfonamide; With pyridine; oxygen; sodium carbonate; copper dichloride; In toluene; at 70 ℃; for 0.25h;

n-octyne; In toluene; at 70 ℃; for 8h;
DOI:10.1021/acs.joc.5b01608

Reference yield:

: 68-34-8
phenyl toluenesulfonamide

: 38761-67-0
1-bromo-1-octyne

: 1116153-63-9
4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

Guidance literature:: With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; In toluene; at 80 ℃; Inert atmosphere;
DOI:10.5012/bkcs.2010.31.03.570

Reference yield: 92.0%

: 1116153-63-9
4-methyl-N-(oct-1-yn-1-yl)-N-phenylbenzenesulfonamide

: 1382470-89-4
4-(methylthio)-5,6-dihydro-2H-pyran-3-carbaldehyde

: C₂₈H₃₅NO₄S₂

Guidance literature:: With bis(norbornadiene)rhodium(l)tetrafluoroborate; bis[2-(diphenylphosphino)phenyl] ether; In acetone; at 55 ℃; for 16h;
DOI:10.1039/c7sc03795c