2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

Base Information

Chemical Name:2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol
CAS No.:132375-34-9
Molecular Formula:C₁₈H₃₀O₄Si
Molecular Weight:338.519
Hs Code.:

Synonyms:2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

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Chemical Property of 2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

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Technology Process of 2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

There total 4 articles about 2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 132375-34-9
2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: 2) camphersulfonic acid / 1) THF, 80 deg C, 4 h, 2) CH₂Cl₂, 25 deg C, 12 h

2: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 °C

3: 1) ozone, 2) NaBH₄ / 1) CH₂Cl₂, -78 deg C, 2 h, 2) MeOH, 0 deg C, 2 h

With 2,6-dimethylpyridine; sodium tetrahydroborate; camphor-10-sulfonic acid; ozone; In dichloromethane;

Reference yield:

: 69739-34-0
t-butyldimethylsiyl triflate

: 132375-34-9
2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 °C

2: 1) ozone, 2) NaBH₄ / 1) CH₂Cl₂, -78 deg C, 2 h, 2) MeOH, 0 deg C, 2 h

With 2,6-dimethylpyridine; sodium tetrahydroborate; ozone; In dichloromethane;

Reference yield:

: 112230-88-3
(E)-4-((4S,5R)-5-Hydroxy-2-phenyl-[1,3]dioxan-4-yl)-but-2-enoic acid methyl ester

: 132375-34-9
2-[(4S,5R)-5-(tert-Butyl-dimethyl-silanyloxy)-2-phenyl-[1,3]dioxan-4-yl]-ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h / 0 °C

2: 1) ozone, 2) NaBH₄ / 1) CH₂Cl₂, -78 deg C, 2 h, 2) MeOH, 0 deg C, 2 h

With 2,6-dimethylpyridine; sodium tetrahydroborate; ozone; In dichloromethane;