HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT

Base Information

Chemical Name:HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT
CAS No.:106209-98-7
Molecular Formula:C₂₇H₂₂BN₆*K
Molecular Weight:480.421
Hs Code.:29331990
Mol file:106209-98-7.mol

Synonyms:Borate(1-),hydrotris(3-phenyl-1H-pyrazolato-N1)-, potassium, (T-4)-; Borate(1-),hydrotris(3-phenyl-1H-pyrazolato-kN1)-, potassium, (T-4)- (9CI); 1H-Pyrazole, 3-phenyl-, boron complex;Potassium [hydrotris(3-phenylpyrazolyl)borate(1-); Potassiumhydridotris(3-phenylpyrazolyl)borate; Potassiumhydrotris(3-phenylpyrazol-1-yl)borate; Potassiumhydrotris(3-phenylpyrazolyl)borate; Potassiumtris[3-phenylpyrazolyl]hydridoborate

Suppliers and Price of HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT 95.00%
5MG
$ 498.29

Total 8 raw suppliers

Chemical Property of HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT

Chemical Property:

Melting Point:267-269 °C
PSA：81.15000
LogP:3.68050

Purity/Quality:

98%min ^*data from raw suppliers

HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Safety Statements: 24/25

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT

There total 1 articles about HYDROTRIS(3-PHENYLPYRAZOL-1-YL)BORATE POTASSIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: potassium borohydride

: 2458-26-6
3-phenylpyrazole

: 106209-98-7
potassium hydrotris(3-phenylpyrazol-1-yl)borate

Guidance literature:: In further solvent(s); heated slowly mixture of 3-phenylpyrazole and KBH4 in anhydrous anisole; heated soln. slowly to reflux; pptn. after 2 days; filtn.; washed; stirring with Celite in THF; filtn.; removal of solvent; elem. anal.;

Reference yield: 77.0%

: iron(II) triflate

: 106209-98-7
potassium hydrotris(3-phenylpyrazol-1-yl)borate

: 128576-17-0
iron(II){hydrotris(3-phenylpyrazol-1-yl)borate}2*CH₂Cl₂*C₆H₁₂

Guidance literature:: In tetrahydrofuran; (N2); addn. of Fe(CF3SO3)2 to soln. of Ktppb in THF; stirring for 2 h; dissoln. in CH2Cl2; addn. of hexane; cooling at -14°C; filtn.; removal of solvent; recrystn.; elem. anal.;

Reference yield: 71.0%

: manganese(II) triflate bis-acetonitrile solvate

: 106209-98-7
potassium hydrotris(3-phenylpyrazol-1-yl)borate

: 128576-18-1
manganese(II){hydrotris(3-phenylpyrazol-1-yl)borate}2*1.4CH₂Cl₂

Guidance literature:: In tetrahydrofuran; addn. of Mn(CF3SO3)2*2MeCN to soln. of Ktppb in THF; stirring for 2 h; removal of solvent under vac.; dissoln. in CH2Cl2 ; addn. of hexane; cooling at -14°C; filtn.; removal of solvent; recrystn.; elem. anal.;