(S,R) 3-benzoyloxy nonane-1,2-diol

Base Information

Chemical Name:(S,R) 3-benzoyloxy nonane-1,2-diol
CAS No.:131157-18-1
Molecular Formula:C₁₆H₂₄O₄
Molecular Weight:280.364
Hs Code.:

Synonyms:(S,R) 3-benzoyloxy nonane-1,2-diol

Suppliers and Price of (S,R) 3-benzoyloxy nonane-1,2-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S,R) 3-benzoyloxy nonane-1,2-diol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S,R) 3-benzoyloxy nonane-1,2-diol

There total 3 articles about (S,R) 3-benzoyloxy nonane-1,2-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (4S)4-((Z)(1R)1-t-butyldiphenylsilyloxy 3-heptenyl) 2,2-dimethyl-1,3-dioxolane

: 131157-18-1
(S,R) 3-benzoyloxy nonane-1,2-diol

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd-C / ethyl acetate / 15 h / 760 Torr

2: 1) Bu₄NF, HOAc, 2) NEt₃ / 1) THF, 28 h, 50 deg C, 2) CH₂Cl₂, RT, 30h

3: 288 mg / 80percent HOAc / 7 h / 45 °C

With tetrabutyl ammonium fluoride; hydrogen; acetic acid; triethylamine; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0040-4020(01)96002-8

Reference yield:

: (4S)4-((1R)1-benzoyloxyheptyl) 2,2-dimethyl 1,3-dioxolane

: 131157-18-1
(S,R) 3-benzoyloxy nonane-1,2-diol

Guidance literature:: With acetic acid; at 45 ℃; for 7h;
DOI:10.1016/S0040-4020(01)96002-8

Reference yield:

: tert-Butyl-[(R)-1-((R)-4,4-dimethyl-[1,3]dioxolan-2-yl)-heptyloxy]-diphenyl-silane

: 131157-18-1
(S,R) 3-benzoyloxy nonane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 1) Bu₄NF, HOAc, 2) NEt₃ / 1) THF, 28 h, 50 deg C, 2) CH₂Cl₂, RT, 30h

2: 288 mg / 80percent HOAc / 7 h / 45 °C

With tetrabutyl ammonium fluoride; acetic acid; triethylamine;
DOI:10.1016/S0040-4020(01)96002-8