2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

Base Information

Chemical Name:2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran
CAS No.:145723-27-9
Molecular Formula:C₁₇H₁₄O₅
Molecular Weight:298.295
Hs Code.:

Synonyms:2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

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Chemical Property of 2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

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Technology Process of 2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

There total 5 articles about 2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 145723-23-5
2-(3-Acetoxyphenyl)-3-methylbenzofuran

: 145723-33-7
2-(3-Acetoxyphenyl)-2,3-dihydro-2-(hydroperoxy)-3-methylenebenzofuran

: 145723-27-9
2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

Guidance literature:: With oxygen; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; at -25 ℃; for 16h; Irradiation;

Reference yield:

: 21535-97-7
3-methyl-benzofuran

: 145723-27-9
2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

Guidance literature:: Multi-step reaction with 4 steps

2: 66 percent / BBr₃ / 0 °C

3: 82 percent / pyridine

4: 20 percent / O₂ / tetraphenylporphine (TPP) / CH₂Cl₂ / 16 h / -25 °C / Irradiation

With pyridine; oxygen; boron tribromide; 5,15,10,20-tetraphenylporphyrin; In dichloromethane;

Reference yield:

: 5961-61-5
3-Methoxyphenylmercuric chloride

: 145723-27-9
2a-(3-Acetoxyphenyl)-2a,7b-dihydro-7b-methyl-1,2-dioxeto<3,4-b>benzofuran

Guidance literature:: Multi-step reaction with 4 steps

2: 66 percent / BBr₃ / 0 °C

3: 82 percent / pyridine

4: 20 percent / O₂ / tetraphenylporphine (TPP) / CH₂Cl₂ / 16 h / -25 °C / Irradiation

With pyridine; oxygen; boron tribromide; 5,15,10,20-tetraphenylporphyrin; In dichloromethane;