Technology Process of C9H9N3O
There total 5 articles about C9H9N3O which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C15H24O5SSi;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
With
sodium azide; water;
In
tetrahydrofuran;
at 70 ℃;
for 21h;
DOI:10.1016/j.tetasy.2012.04.018
- Guidance literature:
-
Multi-step reaction with 5 steps
1: AD-mix-α / Green chemistry
2: thionyl chloride / Green chemistry
3: sodium periodate; ruthenium trichloride / Green chemistry
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 30 h / 20 °C / Green chemistry
5: sodium azide / tetrahydrofuran / 96 h / 70 °C / Green chemistry
With
ruthenium trichloride; sodium periodate; thionyl chloride; sodium azide; AD-mix-α; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
DOI:10.1002/bkcs.10111
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / Green chemistry
2: sodium periodate; ruthenium trichloride / Green chemistry
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 30 h / 20 °C / Green chemistry
4: sodium azide / tetrahydrofuran / 96 h / 70 °C / Green chemistry
With
ruthenium trichloride; sodium periodate; thionyl chloride; sodium azide; tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
DOI:10.1002/bkcs.10111