C₁₅H₂₂O₃

Base Information

Chemical Name:C₁₅H₂₂O₃
CAS No.:955007-44-0
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

C<sub>15</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:C₁₅H₂₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₂O₃

Chemical Property:

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Technology Process of C₁₅H₂₂O₃

There total 1 articles about C₁₅H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 955007-46-2
C₁₆H₂₄O₄

: 955007-44-0
C₁₅H₂₂O₃

Guidance literature:: C₁₆H₂₄O₄; With chloro-trimethyl-silane; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; for 5h; Heating;

With hydrogenchloride; In tetrahydrofuran; for 0.666667h;

diazomethane; In diethyl ether; at 0 ℃; for 0.5h; Further stages.;
DOI:10.1016/j.tetlet.2007.07.163

Reference yield:

: 955007-44-0
C₁₅H₂₂O₃

: 28296-85-7,28400-11-5,52078-92-9,90025-11-9,121350-29-6,121350-30-9
(+/-)-β-acorenol

Guidance literature:: Multi-step reaction with 6 steps

1: 98 percent / 1,3-bis(mesityl)imidazolidin-2-yl[Cl₂Ru(PCy₃)=CHPh] / benzene / 3 h / Heating

2: 100 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760.05 Torr

3: 89 percent / AmO(-)K(+) / benzene / 1 h / 20 °C

4: 90 percent / NaOMe / methanol / 8 h / Heating

5: PTSA / CH₂Cl₂ / 6 h / 20 °C

6: 86 percent / diethyl ether / 3 h / 20 °C

With hydrogen; sodium methylate; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; benzene; 3: Wittig reaction;
DOI:10.1016/j.tetlet.2007.07.163

Reference yield:

: 955007-44-0
C₁₅H₂₂O₃

: 28296-85-7,28400-11-5,52078-92-9,90025-11-9,121350-29-6,121350-30-9
4-epi-α-acorenol

Guidance literature:: Multi-step reaction with 5 steps

1: 98 percent / 1,3-bis(mesityl)imidazolidin-2-yl[Cl₂Ru(PCy₃)=CHPh] / benzene / 3 h / Heating

2: 100 percent / H₂ / Pd/C / methanol / 1 h / 20 °C / 760.05 Torr

3: 89 percent / AmO(-)K(+) / benzene / 1 h / 20 °C

4: PTSA / CH₂Cl₂ / 6 h / 20 °C

5: 85 percent / diethyl ether / 3 h / 20 °C

With hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; benzene; 3: Wittig reaction;
DOI:10.1016/j.tetlet.2007.07.163