3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate
CAS No.:1063596-29-1
Molecular Formula:C₂₆H₂₈Cl₃NO₇S
Molecular Weight:604.936
Hs Code.:

Synonyms:3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

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Chemical Property of 3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

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Technology Process of 3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

There total 1 articles about 3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranose

: 545-06-2
trichloroacetonitrile

: 1063596-29-1
3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol801833n

Reference yield:

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 1063596-29-1
3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

: C₅₂H₅₈O₁₂S

: C₅₂H₅₈O₁₂S

Guidance literature:: methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside; 3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate; In dichloromethane; at 20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol801833n

Reference yield:

: 1063596-29-1
3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate

: 76375-66-1
methyl 2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: 1063596-46-2
methyl (3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

: methyl (3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-β-D-glucopyranosyl)-(1->3)-2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside

Guidance literature:: 3,4-di-O-acetyl-6-O-[(S)-1-phenyl-2-(phenylsulfanyl)ethyl]-2-deoxy-α-D-glucopyranosyl trichloroacetimidate; methyl 2-O-benzyl-4,6-O-benzylidene-α-D-glucopyranoside; In dichloromethane; at 20 ℃; for 0.333333h; Molecular sieve; Inert atmosphere;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -78 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol801833n