phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester

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Chemical Name:phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester
CAS No.:369626-98-2
Molecular Formula:C₃₈H₄₀ClN₅O₈P₂
Molecular Weight:792.165
Hs Code.:

Synonyms:phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester

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Technology Process of phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester

There total 2 articles about phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 990-91-0
dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

: 369626-96-0
2-(2-chloro-6-methylamino-purin-9-ylmethyl)-propane-1,3-diol

: 369626-98-2
phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 20 ℃; for 0.666667h;
DOI:10.1021/jm010082h

Reference yield:

: 369626-94-8
{9-[3-(tert-butyldimethylsilanyloxy)-1-(tert-butyldimethylsilanyloxymethyl)-propyl]-2-chloro-9H-purin-6-yl}-methylamine

: 369626-98-2
phosphoric acid dibenzyl ester 3-(bisbenzyloxyphosphoryloxy)-2-(2-chloro-6-methylaminopurin-9-ylmethyl)propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / aq. AcOH / tetrahydrofuran / 24 h / 50 °C

2: 53 percent / sodium hydride / tetrahydrofuran / 0.67 h / 0 - 20 °C

With sodium hydride; acetic acid; In tetrahydrofuran;
DOI:10.1021/jm010082h