Benzenesulfino-p-toluidide

Base Information

Chemical Name:Benzenesulfino-p-toluidide
CAS No.:5469-22-7
Molecular Formula:C13H13 N O S
Molecular Weight:231.318
Hs Code.:
NSC Number:26917

Synonyms:Benzenesulfino-p-toluidide;5469-22-7;Benzenesulfinamide,N-(4-methylphenyl)-;Benzenesulfinamide, N-(4-methylphenyl)-;NSC26917;N-p-Tolylbenzenesulfinamide;N-(p-Tolyl)-benzenesulfinylamide;WXOCARXEPVPZLP-UHFFFAOYSA-N;NSC-26917;N-(4-Methylphenyl)benzenesulfinamide #

Suppliers and Price of Benzenesulfino-p-toluidide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of Benzenesulfino-p-toluidide

Chemical Property:

Vapor Pressure:2.39E-06mmHg at 25°C
Boiling Point:391.9°C at 760 mmHg
Flash Point:190.8°C
Density:1.25g/cm³
XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:231.07178521
Heavy Atom Count:16
Complexity:230

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)NS(=O)C2=CC=CC=C2

Technology Process of Benzenesulfino-p-toluidide

There total 5 articles about Benzenesulfino-p-toluidide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 624-31-7
4-tolyl iodide

: 16066-31-2,33903-53-6
benzenesulfinamide

: 5469-22-7
N-(p-methylphenyl)benzenesulfinamide

Guidance literature:: With Iron(III) nitrate nonahydrate; potassium phosphate; copper(II) oxide; In N,N-dimethyl-formamide; at 90 ℃; Inert atmosphere;
DOI:10.1016/j.tetlet.2019.151167

Reference yield: 65.0%

: 4972-29-6
benzenesulphinyl chloride

: 106-49-0,12221-03-3
p-toluidine

: 5469-22-7
N-(p-methylphenyl)benzenesulfinamide

Guidance literature:

Reference yield: 48.0%

: 873-55-2
sodium benzenesulfonate

: 106-49-0,12221-03-3
p-toluidine

: 5469-22-7
N-(p-methylphenyl)benzenesulfinamide

Guidance literature:: sodium benzenesulfonate; With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 1h;

p-toluidine; With N-ethyl-N,N-diisopropylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃;
DOI:10.1039/c7ob02028g