(2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

Base Information

Chemical Name:(2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane
CAS No.:82449-88-5
Molecular Formula:C₃₁H₃₂O₄P₂
Molecular Weight:530.54
Hs Code.:

Synonyms:(2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

Suppliers and Price of (2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

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Technology Process of (2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

There total 1 articles about (2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 50622-09-8
2,3-O-isopropylidene-L-threitol

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 82449-88-5
(2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

Guidance literature:: With pyridine; In diethyl ether; at 20 ℃; for 4h;

Reference yield: 45.0%

: 82449-88-5
(2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

: 99436-45-0,94665-48-2
(2R,3R)-1,4-bis(diphenylphosphino)-2,3-dihydroxy-2,3-O-isopropylidnebutane P,P'-dioxide

Guidance literature:: With iodine; at 150 - 160 ℃; for 3.66667h;

Reference yield:

: 82449-88-5
(2S,3S)-2,3-o-isopropylidene-2,3-dihydroxy-1,4-(diphenylphosphinoxy)bitane

: 32305-98-9
(-)-Diop

Guidance literature:: Multi-step reaction with 2 steps

1: 45 percent / I₂ / 3.67 h / 150 - 160 °C

2: 68 percent / trichlorosilane / toluene / 15 h / 70 - 80 °C

With trichlorosilane; iodine; In toluene;