N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

Base Information

Chemical Name:N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide
CAS No.:82082-28-8
Molecular Formula:C₂₁H₁₆Cl₃NO₃S
Molecular Weight:468.788
Hs Code.:

Synonyms:N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

Suppliers and Price of N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

Chemical Property:

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Technology Process of N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

There total 5 articles about N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6628-86-0
5-chloro-2-nitrobenzaldehyde

: 82082-28-8
N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-BuLi / 1.) THF, -78 deg C, 20 min, 2.) THF, -78 deg C, 1 h

2: Jones reagent, acetic acid / diethyl ether / 12 h / Ambient temperature

3: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

4: 88 percent / pyridine / 1.33 h / Heating

5: 1.) MeONa / 1.) MeOH, RT, 1 h , 2.) DMF, 4 h

With pyridine; n-butyllithium; jones reagent; hydrogen; sodium methylate; acetic acid; nickel; In diethyl ether; ethanol;
DOI:10.1021/jm00351a009

Reference yield:

: 82082-25-5
(2,6-dichlorophenyl)(5-chloro-2-nitrophenyl)methanone

: 82082-28-8
N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

2: 88 percent / pyridine / 1.33 h / Heating

3: 1.) MeONa / 1.) MeOH, RT, 1 h , 2.) DMF, 4 h

With pyridine; hydrogen; sodium methylate; nickel; In ethanol;
DOI:10.1021/jm00351a009

Reference yield:

: 875644-89-6
(2-nitro-5-chlorophenyl)(2,6-dichlorophenyl)methanol

: 82082-28-8
N-<4-chloro-2-(2,6-dichlorobenzoyl)phenyl>-N-methyl-4-methylbenzenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: Jones reagent, acetic acid / diethyl ether / 12 h / Ambient temperature

2: 62 percent / H₂ / Raney nickel / ethanol / 8 h / 760 Torr

3: 88 percent / pyridine / 1.33 h / Heating

4: 1.) MeONa / 1.) MeOH, RT, 1 h , 2.) DMF, 4 h

With pyridine; jones reagent; hydrogen; sodium methylate; acetic acid; nickel; In diethyl ether; ethanol;
DOI:10.1021/jm00351a009