4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Base Information

• Chemical Name: 4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate
• CAS No.: 960299-58-5
• Molecular Formula: C₂₀H₁₅F₂NO₃
• Molecular Weight: 355.341

Synonyms:4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Chemical Property of 4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

Chemical Property:

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Technology Process of 4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate

There total 1 articles about 4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

4-Fluorobenzyl bromide (459-46-1) → methyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate (888721-12-8) + 4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate (960299-58-5)

Guidance literature:

methyl-2-oxo-1,2-dihydro-3-pyridinecarbonitrile; With lithium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

4-Fluorobenzyl bromide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 4h;

Reference yield:

4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate (960299-58-5) → 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylic acid hydrochloride

Guidance literature:

4-fluorobenzyl 1-(4-fluorobenzyl)-2-oxo-1,2-dihydropyridine-3-carboxylate; With lithium hydroxide; water; In tetrahydrofuran; methanol; at 20 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; methanol; water; pH=1;

upstream raw materials:

4-Fluorobenzyl bromide

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