1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

Base Information

Chemical Name:1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose
CAS No.:328313-75-3
Molecular Formula:C₁₄H₁₅F₃O₈S₂
Molecular Weight:432.396
Hs Code.:

Synonyms:1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

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Chemical Property of 1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

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Technology Process of 1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

There total 1 articles about 1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 23643-30-3
1,6-anhydro-4-deoxy-2-O-p-toluenesulphonyl-β-D-xylo-hexopyranose

: 358-23-6
trifluoromethylsulfonic anhydride

: 328313-75-3
1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

Guidance literature:: With pyridine; In dichloromethane; at -16 ℃; for 1h;
DOI:10.1135/cccc20001737

Reference yield:

: 328313-75-3
1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

: 53716-80-6
1,6-anhydro-3,4-dideoxy-2-O-p-toluenesulfonyl-β-D-erythro-hex-3-enopyranose

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1135/cccc20001737

Reference yield:

: 328313-75-3
1,6-Anhydro-4-deoxy-2-O-tosyl-3-O-(trifluoromethanesulfonyl)-β-D-xylo-hexopyranose

: 1,6-Anhydro-2,3-dideoxy-4-S-phenyl-4-thio-β-D-erythro-hex-2-enopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 0.75 g / DBU / CH₂Cl₂ / 1 h / 20 °C

2: 99 percent / K₂CO₃ / acetone / 1 h / 20 °C

With potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; acetone;
DOI:10.1135/cccc20001737