3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

Base Information

Chemical Name:3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside
CAS No.:417703-02-7
Molecular Formula:C₂₁H₂₉BrO₈
Molecular Weight:489.36
Hs Code.:

Synonyms:3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

Suppliers and Price of 3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

There total 1 articles about 3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 53207-00-4
1-bromo-2-(bromomethyl)-4,5-dimethoxybenzene

: 2595-05-3
Diacetone D-glucose

: 417703-02-7
3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; at 25 ℃; for 12h;

Reference yield:

: 417703-02-7
3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

: (R)-1-[(3aR,5R,6R,6aR)-6-(2-Bromo-4,5-dimethoxy-benzyloxy)-2,2-dimethyl-tetrahydro-furo[2,3-d][1,3]dioxol-5-yl]-ethane-1,2-diol

Guidance literature:: With acetic acid; at 25 ℃;

Reference yield:

: 417703-02-7
3-O-(2-bromo-4,5-dimethoxybenzyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranoside

: 417703-07-2
5,6-dideoxy-1,2-O-isopropylidene-3-O-(2-bromo-4,5-dimethoxybenzyl)-α-D-ribo-hex-5-enofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: aq. AcOH / 25 °C

2: Ph₃P; I₂; imidazole / toluene / 3 h / Heating

With 1H-imidazole; iodine; acetic acid; triphenylphosphine; In toluene;