Technology Process of C9H9Br2NO2
There total 4 articles about C9H9Br2NO2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
pyridine; hydroxylamine hydrochloride;
at 130 ℃;
for 6h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: aluminum (III) chloride / 3 h / 160 °C / Inert atmosphere
2: sodium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
3: pyridine; hydroxylamine hydrochloride / 6 h / 130 °C / Inert atmosphere
With
pyridine; aluminum (III) chloride; hydroxylamine hydrochloride; sodium carbonate;
In
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere
2: aluminum (III) chloride / 3 h / 160 °C / Inert atmosphere
3: sodium carbonate / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
4: pyridine; hydroxylamine hydrochloride / 6 h / 130 °C / Inert atmosphere
With
pyridine; aluminum (III) chloride; hydroxylamine hydrochloride; sodium carbonate;
In
dichloromethane; N,N-dimethyl-formamide;