2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide

Base Information

Chemical Name:2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide
CAS No.:946088-40-0
Molecular Formula:C₃₁H₃₈N₄O
Molecular Weight:482.669
Hs Code.:

Synonyms:2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide

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Chemical Property of 2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide

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Technology Process of 2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide

There total 2 articles about 2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 946088-32-0
5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-ol

: 88333-03-3,10340-91-7
Benzyl isocyanide

: 107-11-9,30551-89-4
1-amino-2-propene

: 590-86-3
isovaleraldehyde

: 946088-40-0
2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide

Guidance literature:: In toluene; at 110 ℃; for 96h;
DOI:10.1021/jo070706c

Reference yield:

: 104196-99-8,42185-42-2
2-acetyl-hex-5-enoic acid ethyl ester

: 946088-40-0
2-[(allyl)(5-(but-3-enyl)-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-4-methyl-pentanoic acid benzylamide

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / NaOEt / ethanol / 80 °C

2: 71 percent / toluene / 96 h / 110 °C

With sodium ethanolate; In ethanol; toluene;
DOI:10.1021/jo070706c