6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate

Base Information

Chemical Name:6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate
CAS No.:176165-26-7
Molecular Formula:C₃₈H₄₀Cl₃NO₁₈
Molecular Weight:905.091
Hs Code.:

Synonyms:6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate

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Technology Process of 6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate

There total 2 articles about 6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 545-06-2
trichloroacetonitrile

: 6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-D-galactopyranoside

: 176165-26-7
6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate

Guidance literature:: With DCMU; In dichloromethane; for 5h;
DOI:10.1021/jo951914k

Reference yield:

: 176165-24-5
p-methoxyphenyl 6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-β-D-galactopyranoside

: 176165-26-7
6-O-acetyl-2,3-di-O-benzoyl-4-O-(2,3,4,6-tetra-O-acetyl-α-D-galactopyranosyl)-α-D-galactopyranoside trichloroacetylamidate

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / CAN / acetone; H₂O / 0.5 h / Ambient temperature

2: 91 percent / DMU / CH₂Cl₂ / 5 h

With ammonium cerium(IV) nitrate; DCMU; In dichloromethane; water; acetone;
DOI:10.1021/jo951914k