C₃₇H₇₀NO₁₇P

Base Information

Chemical Name:C₃₇H₇₀NO₁₇P
CAS No.:1310568-65-0
Molecular Formula:C₃₇H₇₀NO₁₇P
Molecular Weight:831.933
Hs Code.:

C<sub>37</sub>H<sub>70</sub>NO<sub>17</sub>P

Synonyms:C₃₇H₇₀NO₁₇P

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Chemical Property of C₃₇H₇₀NO₁₇P

Chemical Property:

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Technology Process of C₃₇H₇₀NO₁₇P

There total 12 articles about C₃₇H₇₀NO₁₇P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1310568-58-1
C₂₈H₄₈O₁₂

: 1310568-65-0
C₃₇H₇₀NO₁₇P

Guidance literature:: Multi-step reaction with 5 steps

1: phosphorus tribromide / dichloromethane / 2 h / 0 - 20 °C

2: 2 h / 160 °C

3: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

4: potassium carbonate; potassium iodide / acetone / 48 h / 60 °C

5: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; phosphorus tribromide; potassium carbonate; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 4: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144

Reference yield:

: 1246999-33-6
2-(2-(2-(2-((tert-butoxycarbonyl)amino)ethoxy)ethoxy)ethoxy)ethyl-(4'-methylbenzolsulfonate)

: 1310568-65-0
C₃₇H₇₀NO₁₇P

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / acetone / 48 h / 60 °C

2: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With potassium carbonate; trifluoroacetic acid; potassium iodide; In dichloromethane; acetone; 1: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144

Reference yield:

: 1310568-60-5
C₃₂H₅₇O₁₄P

: 1310568-65-0
C₃₇H₇₀NO₁₇P

Guidance literature:: Multi-step reaction with 3 steps

1: sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / tetrahydrofuran; N,N-dimethyl-formamide / 2 h / 20 °C

2: potassium carbonate; potassium iodide / acetone / 48 h / 60 °C

3: trifluoroacetic acid / dichloromethane / 0 - 20 °C

With sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; trifluoroacetic acid; potassium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetone; 2: Williamson reaction;
DOI:10.1016/j.tetlet.2011.03.144