(S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide

Base Information

Chemical Name:(S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide
CAS No.:114992-64-2
Molecular Formula:C₁₄H₁₅N₅O₄
Molecular Weight:317.304
Hs Code.:

Synonyms:(S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide

Chemical Property:

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Technology Process of (S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide

There total 2 articles about (S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 114992-63-1
(S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>chloroacetamide

: 114992-64-2
(S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide

Guidance literature:: With sodium azide; 18-crown-6 ether; In N,N-dimethyl-formamide; at 70 ℃; for 5h;
DOI:10.1021/jm00128a003

Reference yield:

: 114992-58-4
(S)-5-(aminomethyl)-3-(4-acetylphenyl)-2-oxooxazolidine

: 114992-64-2
(S)-N-<<3-(4-acetylphenyl)-2-oxo-5-oxazolidinyl>methyl>-2-azidoacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / NaOH / H₂O; tetrahydrofuran / 0 - 5 °C

2: 87 percent / NaN₃, 18-crown-6 / dimethylformamide / 5 h / 70 °C

With sodium hydroxide; sodium azide; 18-crown-6 ether; In tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00128a003