C₂₂H₂₀N₂O₂S

Base Information

Chemical Name:C₂₂H₂₀N₂O₂S
CAS No.:1384865-54-6
Molecular Formula:C₂₂H₂₀N₂O₂S
Molecular Weight:376.479
Hs Code.:

C<sub>22</sub>H<sub>20</sub>N<sub>2</sub>O<sub>2</sub>S

Synonyms:C₂₂H₂₀N₂O₂S

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Chemical Property of C₂₂H₂₀N₂O₂S

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Technology Process of C₂₂H₂₀N₂O₂S

There total 4 articles about C₂₂H₂₀N₂O₂S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 109-97-7,30604-81-0
pyrrole

: 156026-71-0
[N-(phenylsulfonyl)-pyrrol-3-yl]-(4-methylphenyl)-methanol

: 1384865-54-6
C₂₂H₂₀N₂O₂S

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jo300810n

Reference yield:

: 16851-82-4
N-phenylsulfonylpyrrole

: 1384865-54-6
C₂₂H₂₀N₂O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / Inert atmosphere

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.25 h / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 1: Friedel Crafts acylation;
DOI:10.1021/jo300810n

Reference yield:

: 874-60-2
4-methyl-benzoyl chloride

: 1384865-54-6
C₂₂H₂₀N₂O₂S

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / Inert atmosphere

2: sodium tetrahydroborate / tetrahydrofuran; methanol / 0.25 h / Inert atmosphere

3: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

With aluminum (III) chloride; sodium tetrahydroborate; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; 1: Friedel Crafts acylation;
DOI:10.1021/jo300810n