10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione

Base Information

• Chemical Name: 10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione
• CAS No.: 1018831-23-6
• Molecular Formula: C₂₅H₂₀N₂O₆
• Molecular Weight: 444.444

Synonyms:10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione

Chemical Property of 10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione

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Technology Process of 10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione

There total 1 articles about 10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 30.0%

Ethyl β-keto-β-(3-indolyl)propionate (52816-02-1) + N-benzyloxymethyl-3,4-dibromomaleimide (102147-52-4) → 10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione (1018831-23-6)

Guidance literature:

Ethyl β-keto-β-(3-indolyl)propionate; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.5h;

N-benzyloxymethyl-3,4-dibromomaleimide; In tetrahydrofuran; at 0 ℃; for 2h; Further stages.;

DOI:10.1016/j.ejmech.2007.03.026

Reference yield: 96.0%

10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione (1018831-23-6) → 10H-2-benzyloxymethyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione (1018831-25-8)

Guidance literature:

With lithium chloride; In N,N-dimethyl-formamide; for 18h; Heating;

DOI:10.1016/j.ejmech.2007.03.026

Reference yield: 94.0%

10H-2-benzyloxymethyl-4-ethoxycarbonyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione (1018831-23-6) → 10H-2-benzyloxymethyl-5-chloro-4-ethoxycarbonyl-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione (1018831-24-7)

Guidance literature:

With phosphorus pentachloride; In N,N-dimethyl-formamide; for 18h; Heating;

DOI:10.1016/j.ejmech.2007.03.026

upstream raw materials:

Ethyl β-keto-β-(3-indolyl)propionate

N-benzyloxymethyl-3,4-dibromomaleimide

Downstream raw materials:

10H-2-benzyloxymethyl-5-chloro-4-ethoxycarbonyl-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione

10H-2-benzyloxymethyl-5-hydroxy-1,3-dihydropyrrolo[3,4-a]carbazole-1,3-dione

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