1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[⁽²⁾H₁₀]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane

Base Information

• Chemical Name: 1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[⁽²⁾H₁₀]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane
• CAS No.: 1158081-97-0
• Molecular Formula: C₄₄H₄₀N₂O₂P₂
• Molecular Weight: 700.682

Synonyms:1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[⁽²⁾H₁₀]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane

Chemical Property of 1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[⁽²⁾H₁₀]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane

Chemical Property:

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Technology Process of 1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[⁽²⁾H₁₀]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane

There total 1 articles about 1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[⁽²⁾H₁₀]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

[(2)H10]-2-(diphenylphosphino)benzoic acid (1158081-71-0) + [(1R,2R)-N-(2-aminocyclohexenyl)]-2-(diphenylphosphanoyl)benzamide (291286-34-5) → 1(R),2(R)-1-N-[2'-(diphenylphosphino)benzoyl]-2-N-{[(2)H10]-2'-(diphenylphosphino)benzoyl}diaminocyclohexane (1158081-97-0)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Inert atmosphere;

DOI:10.1021/ja8099757

upstream raw materials:

[⁽²⁾H₁₀]-2-(diphenylphosphino)benzoic acid

[(1R,2R)-N-(2-aminocyclohexenyl)]-2-(diphenylphosphanoyl)benzamide

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