tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

Base Information

Chemical Name:tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate
CAS No.:866831-53-0
Molecular Formula:C₁₈H₂₈N₂O₃
Molecular Weight:320.432
Hs Code.:

Synonyms:tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

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Chemical Property of tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

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Technology Process of tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

There total 1 articles about tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 103-82-2
phenylacetic acid

: 79069-14-0,106391-87-1
tert-butyl [(1R)-1-(hydroxymethyl)-2-methylpropyl]carbamate

: 866831-53-0
tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

Guidance literature:: tert-butyl [(1R)-1-(hydroxymethyl)-2-methylpropyl]carbamate; With methanesulfonyl chloride; triethylamine; In dichloromethane; at 20 ℃;

With sodium azide; In N,N-dimethyl-formamide; at 80 ℃;

phenylacetic acid; With hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium 10% on activated carbon; more than 3 stages;

Reference yield:

: 866831-53-0
tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

: 866831-55-2
N-[(2R)-2-amino-3-methylbutyl]-2-phenylacetamide

Guidance literature:: tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate; With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 2h;

With sodium hydroxide; In dichloromethane; water;

Reference yield:

: 866831-53-0
tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate

: 121-17-5
2-chloro-3-nitro-5-trifluoromethylbenzene

: 1224977-13-2
N-((2R)-3-methyl-2-{[2-nitro-4-(trifluoromethyl)phenyl]amino}butyl)-2-phenylacetamide

Guidance literature:: tert-butyl ((1R)-2-methyl-1-{[(phenylacetyl)amino]methyl}propyl)carbamate; With hydrogenchloride; In 1,4-dioxane;

2-chloro-3-nitro-5-trifluoromethylbenzene; With potassium carbonate; In water; N,N-dimethyl-formamide; at 40 ℃;