Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

Base Information

Chemical Name:Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester
CAS No.:185021-15-2
Molecular Formula:C₁₆H₂₄FNO₄SSi
Molecular Weight:373.521
Hs Code.:

Synonyms:Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

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Chemical Property of Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

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Technology Process of Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

There total 3 articles about Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 185021-12-9
Diethyl-carbamic acid (E)-2-fluoro-2-phenylsulfanyl-1-trimethylsilanyl-vinyl ester

: 185021-15-2
Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 12h;
DOI:10.1016/0040-4039(96)01877-1

Reference yield:

: 143366-88-5
2,2-diflouoro-1-(N,N-diethylcarbamoyloxy)-1-(trimethylsilyl)ethene

: 185021-15-2
Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / NaH, DMPU / tetrahydrofuran / 8 h / Heating

2: 76 percent / m-CPBA / CH₂Cl₂ / 12 h

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4039(96)01877-1

Reference yield:

: 171617-27-9
C₇H₁₀F₂LiNO₂

: 185021-15-2
Diethyl-carbamic acid (E)-2-benzenesulfonyl-2-fluoro-1-trimethylsilanyl-vinyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / -78 - -30 °C

2: 87 percent / NaH, DMPU / tetrahydrofuran / 8 h / Heating

3: 76 percent / m-CPBA / CH₂Cl₂ / 12 h

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium hydride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0040-4039(96)01877-1