Technology Process of C37H50N2O4
There total 7 articles about C37H50N2O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
p-toluenesulfonyl chloride;
In
pyridine; water;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Bis(2,6-dimethylphenyl) hydrogen phosphate; diethylzinc / dichloromethane / 0.5 h / -20 - 0 °C
1.2: 4.5 h / 20 °C
2.1: hydrogen / palladium hydroxide on carbon / ethyl acetate; toluene / 1 h
2.2: 1 h
3.1: aluminum tri-tert-butoxide; butanone / toluene / 16 h / 75 °C
3.2: 3.5 h / 20 °C
4.1: dmap; triethylamine / tetrahydrofuran; dichloromethane / 1 h / 20 °C
5.1: N-methylhydroxyamine hydrochloride; sodium acetate / ethanol / 6 h / 70 °C
6.1: p-toluenesulfonyl chloride / pyridine; water / 0.5 h / 20 °C
With
dmap; Bis(2,6-dimethylphenyl) hydrogen phosphate; N-methylhydroxyamine hydrochloride; hydrogen; diethylzinc; sodium acetate; aluminum tri-tert-butoxide; triethylamine; p-toluenesulfonyl chloride; butanone;
palladium hydroxide on carbon;
In
tetrahydrofuran; pyridine; ethanol; dichloromethane; water; ethyl acetate; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: hydrogen / palladium hydroxide on carbon / ethyl acetate; toluene / 1 h
1.2: 1 h
2.1: aluminum tri-tert-butoxide; butanone / toluene / 16 h / 75 °C
2.2: 3.5 h / 20 °C
3.1: dmap; triethylamine / tetrahydrofuran; dichloromethane / 1 h / 20 °C
4.1: N-methylhydroxyamine hydrochloride; sodium acetate / ethanol / 6 h / 70 °C
5.1: p-toluenesulfonyl chloride / pyridine; water / 0.5 h / 20 °C
With
dmap; N-methylhydroxyamine hydrochloride; hydrogen; sodium acetate; aluminum tri-tert-butoxide; triethylamine; p-toluenesulfonyl chloride; butanone;
palladium hydroxide on carbon;
In
tetrahydrofuran; pyridine; ethanol; dichloromethane; water; ethyl acetate; toluene;